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    3-Deoxyaconitine
    3-Deoxyaconitine
    Information
    CAS No. 3175-95-9 Price $288 / 20mg
    Catalog No.CFN90660Purity>=98%
    Molecular Weight629.74Type of CompoundAlkaloids
    FormulaC34H47NO10Physical DescriptionPowder
    Download     COA    MSDSSimilar structuralComparison (Web)
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    Biological Activity
    Description: 3-Deoxyaconitine has toxicity.
    3-Deoxyaconitine Description
    Source: The roots of Aconitum kusnezoffii Reichb.
    Solvent: Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
    Storage: Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to 24 months(2-8C).

    Wherever possible, you should prepare and use solutions on the same day. However, if you need to make up stock solutions in advance, we recommend that you store the solution as aliquots in tightly sealed vials at -20C. Generally, these will be useable for up to two weeks. Before use, and prior to opening the vial we recommend that you allow your product to equilibrate to room temperature for at least 1 hour.

    Need more advice on solubility, usage and handling? Please email to: service@chemfaces.com

    After receiving: The packaging of the product may have turned upside down during transportation, resulting in the natural compounds adhering to the neck or cap of the vial. take the vial out of its packaging and gently shake to let the compounds fall to the bottom of the vial. for liquid products, centrifuge at 200-500 RPM to gather the liquid at the bottom of the vial. try to avoid loss or contamination during handling.
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    Recently, ChemFaces products have been cited in many studies from excellent and top scientific journals

    Cell. 2018 Jan 11;172(1-2):249-261.e12.
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    Calculate Dilution Ratios(Only for Reference)
    1 mg 5 mg 10 mg 20 mg 25 mg
    1 mM 1.588 mL 7.9398 mL 15.8796 mL 31.7591 mL 39.6989 mL
    5 mM 0.3176 mL 1.588 mL 3.1759 mL 6.3518 mL 7.9398 mL
    10 mM 0.1588 mL 0.794 mL 1.588 mL 3.1759 mL 3.9699 mL
    50 mM 0.0318 mL 0.1588 mL 0.3176 mL 0.6352 mL 0.794 mL
    100 mM 0.0159 mL 0.0794 mL 0.1588 mL 0.3176 mL 0.397 mL
    * Note: If you are in the process of experiment, it's need to make the dilution ratios of the samples. The dilution data of the sheet for your reference. Normally, it's can get a better solubility within lower of Concentrations.
    Protocol
    Structure Identification:
    Acta Crystallogr Sect E Struct Rep Online. 2010 May 15;66(Pt 6):o1342.
    3-Deoxyaconitine from the root of Aconitum Carmichaeli Debx.[Pubmed: 21579431]

    METHODS AND RESULTS:
    3-Deoxyaconitine:8β-acet-oxy-14α-benzo-yloxy-N-ethyl-13β,15α-dihydr-oxy-1α,6α,16β-trimeth-oxy-4β-methoxy-methyl-eneaconitane), C(34)H(47)NO(10), is a typical aconitine-type C(19)-diterpenoid alkaloid, and was isolated from the roots of the Aconitum carmichaeli Debx. The mol-ecule has an aconitine carbon skeleton with four six-membered rings and two five-membered rings, whose geometry is similar to these observed in other C(19)-diterpenoid alkaloids; both of five-membered rings have the envelope configurations and the six-membered N-containing heterocyclic ring displays a chair conformation. Intra-molecular O-H⋯O hydrogen bonding occurs.
    CONCLUSIONS:
    Weak inter-molecular C-H⋯O hydrogen bonding is observed in the crystal structure.
    Chinese Traditional Patent Medicine , 2011 , 33 (3) :479-482.
    Determination of aconitine and 3-deoxyaconitine in fried samples of Aconitum pendulum Busch by HPLC[Reference: WebLink]
    To analyze the influences on the contents of aconitine and 3-Deoxyaconitine in Aconitum pendulum Busch by different processing methods used in Tibetan medicine,Qiang medicine and Hui medicine,and to observe the relativity between processing and toxicity.
    METHODS AND RESULTS:
    The determination was performed by HPLC,and Kromasil C18 column(250 mm×4.6 mm,5 μm) was used with the mobile phase being methanol:water:trieth-ylamine(95:5:0.3),flow rate was 1.0 mL/min,the column temperature was set at 25 ℃,detection wave-length was set at 235 nm.All the contents of aconitine and 3-Deoxyaconitine in A.pendulum Busch samples decreased after being fried.It showed that temperature was the main factor in decomposing the dibasic acid structures of aconitine and reducing toxicity.
    CONCLUSIONS:
    All chromatograph peaks could be well separated,and the method is very stable.And among all the methods,the processing used in Tibetan medicine is much more scientific and effective.