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Sipeimine-3-beta-D-glucoside
Sipeimine-3-beta-D-glucoside
ChemFaces products have been cited in many studies from excellent and top scientific journals
Product Name Sipeimine-3-beta-D-glucoside
Price: $298 / 20mg
CAS No.: 67968-40-5
Catalog No.: CFN91848
Molecular Formula: C33H53NO8
Molecular Weight: 591.8 g/mol
Purity: >=98%
Type of Compound: Alkaloids
Physical Desc.: Powder
Source: The bulbus of Fritillaria thunbergii Miq.
Solvent: DMSO, Pyridine, Methanol, Ethanol, etc.
Download: COA    MSDS
Similar structural: Comparison
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Size /Price /Stock 10 mM * 1 mL in DMSO / $139.5 / In-stock
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Related Screening Libraries
Size /Price /Stock 10 mM * 100 uL in DMSO / Inquiry / In-stock
10 mM * 1 mL in DMSO / Inquiry / In-stock
Related Libraries
Biological Activity
Description: Reference standards.
Sipeimine-3-beta-D-glucoside Description
Source: The bulbus of Fritillaria thunbergii Miq.
Solvent: DMSO, Pyridine, Methanol, Ethanol, etc.
Storage: Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to 24 months(2-8C).

Wherever possible, you should prepare and use solutions on the same day. However, if you need to make up stock solutions in advance, we recommend that you store the solution as aliquots in tightly sealed vials at -20C. Generally, these will be useable for up to two weeks. Before use, and prior to opening the vial we recommend that you allow your product to equilibrate to room temperature for at least 1 hour.

Need more advice on solubility, usage and handling? Please email to: service@chemfaces.com

After receiving: The packaging of the product may have turned upside down during transportation, resulting in the natural compounds adhering to the neck or cap of the vial. take the vial out of its packaging and gently shake to let the compounds fall to the bottom of the vial. for liquid products, centrifuge at 200-500 RPM to gather the liquid at the bottom of the vial. try to avoid loss or contamination during handling.
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Recently, ChemFaces products have been cited in many studies from excellent and top scientific journals

Cell. 2018 Jan 11;172(1-2):249-261.e12.
doi: 10.1016/j.cell.2017.12.019.
IF=36.216(2019)

PMID: 29328914

Cell Metab. 2020 Mar 3;31(3):534-548.e5.
doi: 10.1016/j.cmet.2020.01.002.
IF=22.415(2019)

PMID: 32004475

Mol Cell. 2017 Nov 16;68(4):673-685.e6.
doi: 10.1016/j.molcel.2017.10.022.
IF=14.548(2019)

PMID: 29149595

ACS Nano. 2018 Apr 24;12(4): 3385-3396.
doi: 10.1021/acsnano.7b08969.
IF=13.903(2019)

PMID: 29553709

Nature Plants. 2016 Dec 22;3: 16206.
doi: 10.1038/nplants.2016.205.
IF=13.297(2019)

PMID: 28005066

Sci Adv. 2018 Oct 24;4(10): eaat6994.
doi: 10.1126/sciadv.aat6994.
IF=12.804(2019)

PMID: 30417089
Calculate Dilution Ratios(Only for Reference)
1 mg 5 mg 10 mg 20 mg 25 mg
1 mM 1.6898 mL 8.4488 mL 16.8976 mL 33.7952 mL 42.244 mL
5 mM 0.338 mL 1.6898 mL 3.3795 mL 6.759 mL 8.4488 mL
10 mM 0.169 mL 0.8449 mL 1.6898 mL 3.3795 mL 4.2244 mL
50 mM 0.0338 mL 0.169 mL 0.338 mL 0.6759 mL 0.8449 mL
100 mM 0.0169 mL 0.0845 mL 0.169 mL 0.338 mL 0.4224 mL
* Note: If you are in the process of experiment, it's need to make the dilution ratios of the samples. The dilution data of the sheet for your reference. Normally, it's can get a better solubility within lower of Concentrations.
Protocol
Structure Identification:
Chinese Journal of Experimental Traditional Medical Formulae, 2013.
Determination of Pinocembrin,Cardamonin,Sipeimine and Sipeimine-3β-D-glucoside in Houzao Niuhuangsan by HPLC-ELSD.[Reference: WebLink]
To develop an HPLC-ELSD method for determination of the content of pinocembrin,cardamonin,sipeimine and sipeimine-3β-D-glucoside(Sipeimine-3-beta-D-glucoside) in Houzao Ninhuangsan(HZNHS).
METHODS AND RESULTS:
An Hypersil C18column was used as the chromatographic column,the flow rate was 0.9 mL·min-1.The mobile phase for pinocembrin and cardamonin consisted of methanol(A) and 0.5% phosphoric acid solution(B); the UV detection wavelength was at 300 nm.The mobile phase for sipeimine and sipeimine-3β-D-glucoside consisted of acetonitrile-water-diethylamine(65∶ 35∶ 0.5).The temperature of drift tube was set at 80 ℃,and the gas flow(N2) was set at 2.3 SLPM·min-1. There was a good linear relationship between the concentration of pinocembrin,cardamonin and peak area value when the concentrations of pinocembrin and cardamonin were within the range of 0.052 7-1.054 μg(r = 0.999 4),0.036 2-0.724 0 μg(r = 0.999 8).The average recovery were97.14%(RSD 1.10%) and 97.64%(RSD 1.39%).There was a good linear relationship when the concentrations of sipeimine and sipeimine-3β-D-glucoside were within the range of 0.057 1-1.142 μg(r = 0.9991),0.081 3-1.626 μg(r = 0.999 5).The average recovery was 97.55%(RSD 1.75%) and 98.09%(RSD1.80%).
CONCLUSIONS:
The method was accurate,sensitive,reproducible and may be used in the determination of pinocembrin,cardamonin,sipeimine and sipeimine-3β-D-glucoside in HZNHS.
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